General antonyms:
* Enslave
* Oppress
* Conquer
* Subjugate
* Imprison
* Restrict
* Control
* Bind
Antonyms related to specific contexts:
* Capture (instead of liberating a prisoner)
* Confiscate (instead of liberating property)
* Suppress (instead of liberating speech or expression)
* Restrict (instead of liberating movement or access)
The best antonym will depend on the specific situation and what you are trying to convey.